| Abstract |
|
| 1.0 |
Introduction |
2 |
| 2.0 |
Objective |
2 |
| 3.0 |
Summary and Conclusions |
3 |
| |
3.1 |
Task 1 - Project Work Plan |
3 |
| 3.2 |
Task 2 - Slurry Catalyst
Development |
3 |
| |
3.2.1 |
Sub-Task 2a - Background Studies |
3 |
| 3.2.2 |
Sub-Task 2b - Bench Scale Reactor
Set-Up |
3 |
| 3.2.3 |
Sub-Task 2c - Catalyst
Preparation and Slurry Reactor Testing |
4 |
| 3.2.4 |
Sub-Task 2d - Metal Clust
Catalyst Preparation and Screening Tests |
4 |
| 3.3 |
Task 3 - Slurry Reactor Design
Studies |
4 |
| 3.4 |
Task 4 - Pilot Plant Facility
Design |
5 |
| 4.0 |
Acknowledgement |
5 |
| 5.0 |
Results and Discussion |
5 |
| |
5.1 |
Task 1 - Project Work Plan |
5 |
| 5.2 |
Task 2 - Slurry Catalyst
Development |
5 |
| |
5.2.1 |
Sub-Task 2a - Background Studies |
5 |
| 5.2.2 |
Sub-Task 2b - Bench Scale Reactor
Set-Up |
5 |
| 5.2.3 |
Sub-Task 2c - Catalyst
Preparation and Slurry Reactor Testing |
6 |
| 5.2.4 |
Sub-Task 2d - Metal Cluster
Catalyst Preparation and Screening Tests |
8 |
| 5.3 |
Task 3 - Slurry Reactor Design
Studies |
8 |
| |
5.3.1 |
5" Cold Flow Simulator |
8 |
| 6.0 |
Experimental |
10 |
| |
6.1 |
Task 1 - Project Work Plan |
10 |
| 6.2 |
Task 2 - Slurry Catalyst
Development |
10 |
| |
6.2.1 |
Sub-Task 2a - Background Studies |
10 |
| 6.2.2 |
Sub-Task 2b - Bench Scale Reactor
Set-Up |
10 |
| 6.2.3 |
Sub-Task 2c - Catalyst
Preparation and Slurry Reactor Testing |
15 |
| 6.2.4 |
Sub-Task 2d - Metal Clust
Catalyst Preparation and Screening Tests |
16 |
| 6.3 |
Task 3 - Slurry Reactor Design
Studies |
16 |
| |
6.3.1 |
5" Cold Flow Simulator |
16 |
| 7.0 |
References |
20 |
| 8.0 |
Figures |
21 |
| 9.0 |
Tables |
38 |
| |
|
| LIST OF FIGURES |
|
| Figure 1 -
Hydrocarbon Weight Distribution - 5879-9-B - 23/27 |
21 |
| Figure 2 -
Hydrocarbon Molar Distribution – 5870-9-B – 23/27 |
23 |
|
Figure 3 – Hydrocarbon Schulz-Flory
Distribution – 5870-9-B –23/27 |
24 |
| Figure 37 – Gas
Holdup – 5” Cold Flow Simulator |
25 |
| Figure 38 – Test
Sample Aqueous Phase Analysis |
26 |
| Figure 39 – Test
Sample Liquid Phase Hydrocarbon Analysis |
27 |
| Figure 40 – Data
Organization on Disk |
28 |
| Figure 41 – Test
Sample – Compiled Gas Product Distribution |
29 |
| Figure 42 – Test
Sample (from Figure 39) – Compiled Liquid Phase Organic Analysis |
30 |
| Figure 43 – Test
Sample (from Figure 38) – Compiled Oxygenate Distribution |
31 |
| Figure 44 – Test
Sample (from Figures 41 and 42) – Hydrocarbon Wt% |
32 |
| Figure 45 – Test
Sample (from Figures 41 and 42) – Hydrocarbon Distribution in Mol% |
33 |
| Figure 46 – Test
Sample Schulz-Flory Distribution Plot |
34 |
| Figure 47 – Process
Flow Diagram for 5” Slurry Column |
35 |
| Figure 48 – Eddy
Control Basket |
36 |
| |
|
| LIST OF TABLES |
|
| Table 1 – Process and
Conversion Data – 5870-9-B |
37 |
| Table 2 – Hydrocarbon
Product Distribution – Run 5878-9-B |
39 |
| Table 3 – Oxygenates
Product Distribution – Run 5870-9-B |
40 |
| Table 22 – Gas
Holdup, 5” Cold Flow Simulator |
41 |
| Table 23 – Foam Tests
Summary |
42 |
