| Abstract |
2 |
| Executive Summary |
3 |
| Introduction |
4 |
| Objectives |
4 |
| Engineering and Modifications |
5 |
| |
New Internal Heat Exchanger for 27.10 Reactor |
5 |
| Modifications to Utility Oil System |
5 |
| Process Description |
56 |
| Catalyst-wax Separation System |
6 |
| Analytical Set-up |
6 |
| Hazards Reviews |
8 |
| Environmental Reviews |
8 |
| Reactor Temperature Stability |
8 |
| Catalyst Development |
9 |
| |
Activity Tests |
10 |
| Sedimentation Tests |
10 |
| Catalyst Scale-up |
11 |
| Catalyst Activation at CAER |
12 |
| Cross-Flow Filter Test |
13 |
| Catalyst Qualification |
14 |
| Starting Slurry Medium |
14 |
| Demonstration Run Plan |
14 |
| Results and Discussion |
14 |
| |
Catalyst Activation (F-T II) |
15 |
| Process Variable Study (F-T II) |
16 |
| Analytical/Autoclave Investigations |
17 |
| Catalyst Activation (F-T IIA) |
17 |
| Mass Balance |
19 |
| Alpha Estimate |
19 |
| Reactor Temperature Profile |
19 |
| Pilot Plant Results from Literature |
20 |
| Heat Transfer Coefficients Estimate |
20 |
| Conclusions and Recommendations |
21 |
| Future Plans |
22 |
| Acknowledgements |
22 |
| References |
23 |
| Appendix |
Volume II |
|
A |
Reactor Temperature Stability |
|
|
B |
Mott Cross-flow Filter Test for F-T II |
|
C |
Fischer-Tropsch II Run Authorizations |
|
D |
Fischer-Tropsch II Run Chronology |
|
E |
Liquid Compositions |
|
F |
F-T II/IIA Demonstration Mass Balances |