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Return to DOE Report Table of Contents
Determination of Alcohols in Engine Lubricants - 1981
Frank M.
Newman
Kenneth B. Jones
Southwest
Research Institute
In this pdf format, this document has 21 pages and is
758kb
Table of Contents
| I |
INTRODUCTION |
5 |
| II |
APPROACH |
5 |
| III |
EXPERIMENTAL |
6 |
| |
A |
Instrumentation |
6 |
| B |
Calibration |
9 |
| C |
Sample Prepraration |
|
| IV |
APPLICATION |
12 |
| V |
DISCUSSION |
12 |
| VI |
CONCLUSIONS |
16 |
| VII |
LIST OF REFERENCES |
16 |
| |
| LIST OF ILLUSTRATIONS |
| 1 |
GC Column Configuration |
6 |
| 2 |
Stripper Column Retention of Normal
Hydrocarbons |
8 |
| 3 |
Chromatogram Showing Retention Times of
Alcohols |
9 |
| 4 |
Typical Chromatogram of Calibration Standard |
10 |
| 5 |
Chromatogram of 700 ppm Methanol Standard |
10 |
| 6 |
Response Factor Repeatability |
13 |
| 7 |
Chromatogram of Engine Oil |
14 |
| 8 |
Chromatogram of Engine Oil Sample |
14 |
| 9 |
Chromatogram of Engine Oil Sample - Methanol
Undetected |
15 |
| 10 |
Temperature - Programmed Chromatogram of
Alcohol Composites |
15 |
| |
| LIST OF TABLES |
|
Operating Parameters |
7 |
|
Calculation Method |
11 |
|
Internal Standard/ Analyte Ratio |
13 |
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